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Dye penetrant inspection (DPI), also called liquid = penetrant=20 inspection (LPI) or penetrant testing (PT), is = a widely=20 applied and low-cost inspection method used to locate surface-breaking = defects=20 in all non-porous materials = (metals,=20 plastics, or ceramics). The penetrant may be applied to all non-ferrous=20 materials and ferrous materials, although for ferrous components magnet= ic-particle=20 inspection is often used instead for its subsurface detection = capability.=20 LPI is used to detect casting, forging and welding surface defects such = as=20 hairline cracks, surface porosity,=20 leaks in new products, and fatigue=20 cracks on in-service components.
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The oil and whiting method used in the railroad industry in the early = 1900's=20 was the first recognized use of the principles of penetrants to detect = cracks.=20 The oil and whiting method used an oil solvent for cleaning followed by = the=20 application of a whiting or chalk coating, which absorbed oil from the = cracks=20 revealing their locations. Soon a dye was added to the liquid. By the = 1940's,=20 fluorescent or visible dye was added to the oil used to penetrate test=20 objects.
Experience showed that temperature and soak time were important. This = started=20 the practice of written instructions to provide standard, uniform = results. The=20 use of written procedures has evolved, giving the ability for design = engineers=20 and manufacturers to get the high standard results from any properly = trained and=20 certified liquid penetrant testing technician.
DPI is based upon capillary=20 action, where low surface tension fluid penetrates into clean and = dry=20 surface-breaking discontinuities. Penetrant may be applied to the test = component=20 by dipping, spraying, or brushing. After adequate penetration time has = been=20 allowed, the excess penetrant is removed, a developer is applied. The = developer=20 helps to draw penetrant out of the flaw where a invisible indication = becomes=20 visible to the inspector. Inspection is performed under ultraviolet or = white=20 light, depending upon the type of dye used - fluorescent or=20 nonfluorescent (visible).
Penetrants are classified into sensitivity levels. Visible penetrants = are=20 typically red in color, and represent the lowest sensitivity. = Fluorescent=20 penetrants contain two or more dyes that fluoresce when excited by ultraviolet (UV-A) = radiation=20 (also known as black light). Since Fl= uorescent=20 penetrant inspection is performed in a darkened environment, and the = excited=20 dyes emit brilliant yellow-green light that contrasts strongly against = the dark=20 background, this material is more sensitive to small defects.
When selecting a sensitivity level one must consider many factors, = including=20 the environment under which the test will be performed, the surface = finish of=20 the specimen, and the size of defects sought. One must also assure that = the test=20 chemicals are compatible with the sample so that the examination will = not cause=20 permanent staining, or degradation. This technique can be quite = portable,=20 because in its simplest form the inspection requires only 3 aerosol = spray cans,=20 some lint free clothes, and adequate visible light. Stationary systems = with=20 dedicated application, wash, and development stations, are more costly = and=20 complicated, but result in better sensitivity and higher samples=20 through-put.
Below are the main steps of Liquid Penetrant Inspection:
1. Pre-cleaning:
The test surface is cleaned to remove any dirt, paint, oil, grease or = any=20 loose scale that could either keep penetrant out of a defect, or cause=20 irrelevant or false indications. Cleaning methods may include solvents, alkaline = cleaning=20 steps, vapor=20 degreasing, or media blasting. The end goal of this step is a clean = surface=20 where any defects present are open to the surface, dry, and free of=20 contamination. Note that if media blasting is used, it may "work over" = small=20 discontinuities in the part, and an etching bath is recommended as a = post-bath=20 treatment.
2. Application of Penetrant:
The penetrant is then applied to the surface of the item being = tested. The=20 penetrant is allowed "dwell time" to soak into any flaws (generally 5 to = 30=20 minutes). The dwell time mainly depends upon the penetrant being used, = material=20 being testing and the size of flaws sought. As expected, smaller flaws = require a=20 longer penetration time. Due to their incompatible nature one must be = careful=20 not to apply solvent-based penetrant to a surface which is to be = inspected with=20 a water-washable penetrant.
3. Excess Penetrant Removal:
The excess penetrant is then removed from the surface. The removal = method is=20 controlled by the type of penetrant used. Water-washable, = solvent-removable, lipophilic=20 post-emulsifiable, or hydrophilic=20 post-emulsifiable are the common choices. Emulsifiers = represent the=20 highest sensitivity level, and chemically interact with the oily = penetrant to=20 make it removable with a water spray. When using solvent remover and = lint-free=20 cloth it is important to not spray the solvent on the test surface = directly,=20 because this can remove the penetrant from the flaws. If excess = penetrant is not=20 properly removed, once the developer is applied, it may leave a = background in=20 the developed area that can mask indications or defects. In addition, = this may=20 also produce false indications severely hindering your ability to do a = proper=20 inspection.
4. Application of Developer:
After excess penetrant has been removed a white developer is applied = to the=20 sample. Several developer types are available, including: non-aqueous=20 wet developer, dry powder, water suspendable, and water soluble. = Choice of=20 developer is governed by penetrant compatibility (one can't use = water-soluble or=20 suspendable developer with water-washable penetrant), and by inspection=20 conditions. When using non-aqueous wet developer (NAWD) or dry powder, = the=20 sample must be dried prior to application, while soluble and suspendable = developers are applied with the part still wet from the previous step. = NAWD is=20 commercially available in aerosol spray cans, and may employ acetone, isopropyl = alcohol, or=20 a propellant that is a combination of the two. Developer should form a=20 semi-transparent, even coating on the surface.
The developer draws penetrant from defects out onto the surface to = form a=20 visible indication, commonly known as bleed-out. Any areas that = bleed-out can=20 indicate the location, orientation and possible types of defects on the = surface.=20 Interpreting the results and characterizing defects from the indications = found=20 may require some training and/or experience [the indication size is not = the=20 actual size of the defect]
5. Inspection:
The inspector will use visible light with adequate intensity (100 foot-candles or = 1100 lux is = typical) for=20 visible dye penetrant. Ultraviolet (UV-A) radiation of adequate = intensity (1,000=20 micro-watts per centimeter squared is common), along with low ambient = light=20 levels (less than 2 foot-candles) for fluorescent penetrant = examinations.=20 Inspection of the test surface should take place after a 10 minute = development=20 time. This time delay allows the blotting action to occur. The inspector = may=20 observe the sample for indication formation when using visible dye. It = is also=20 good practice to observe indications as they form because the = characteristics of=20 the bleed out are a significant part of interpretation characterization = of=20 flaws.
6. Post Cleaning:
The test surface is often cleaned after inspection and recording of = defects,=20 especially if post-inspection coating processes are scheduled.
The main advantages of DPI are the speed of the test and the low = cost.=20 Disadvantages include the detection of only surface flaws, skin = irritation, and=20 the inspection should be on a smooth clean surface where excessive = penetrant can=20 be removed prior to being developed. Conducting the test on rough = surfaces,=20 such-as as-welded welds, will make it difficult to remove any excessive=20 penetrant and could result in false indications. Water-washable = penetrant should=20 be considered here if no other option is available. Also, on certain = surfaces a=20 great enough color contrast cannot be achieved or the dye will stain the = workpiece.[1]
Limited training is required for the operator =E2=80=94 although = experience is quite=20 valuable. Proper cleaning is necessary to assure that surface = contaminants have=20 been removed and any defects present are clean and dry. Some cleaning = methods=20 have been shown to be detrimental to test sensitivity, so acid etching = to remove=20 metal smearing and re-open the defect may be necessary.[citation=20 needed]